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Standard Test Methods for Chemical and Mass Spectrometric Analysis of Nuclear-Grade Gadolinium Oxide (Gd2O3) Powder
1.1 These test methods cover procedures for the chemical and mass spectrometric analysis of nuclear-grade gadolinium oxide powders to determine compliance with specifications.
1.2 The analytical procedures appear in the following order:
| Sections | |
| Carbon by Direct Combustion | |
| C1408 Test Method for Carbon (Total) in Uranium Oxide Powders and Pellets By Direct Combustion-Infrared Detection Method | |
| Total Chlorine and Fluorine by Pyrohydrolysis Ion Selective Electrode | |
| C1502 Test Method for Determination of Total Chlorine and Fluorine in Uranium Dioxide and Gadolinium Oxide | |
| Loss of Weight on Ignition | 7-13 |
| Sulfur by Combustion | |
| Impurity Elements by a Spark-Source Mass Spectrographic | |
| C761 Test Methods for Chemical, Mass Spectrometric, Spectrochemical,Nuclear, and Radiochemical Analysis of Uranium Hexafluoride | |
| C1287 Test Method for Determination of Impurities In Uranium Dioxide By Inductively Coupled Plasma Mass Spectrometry | |
| Gadolinium Content in Gadolinium Oxide by Impurity Correction | 14-17 |
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 5. 7.1 This test method covers the loss-on-ignition of volatile constituents from nuclear-grade gadolinium oxide (Gd2O3) powder. 14.1 The percent gadolinium oxide content of powders, exclusive of volatiles, is determined by calculation after the material has been analyzed to determine the total impurities.
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